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Publication no. C-2004-0324-05R
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ARTICLE
Physicochemical Properties of Maize Starch Obtained from Intermittent Milling
and Dynamic Steeping (IMDS) Under Various Steeping Conditions.
E. A. Brandemarte (1), C. M. L. Franco (2), and J. F. Lopes-Filho (2,3). (1)
Former graduate fellow. (2) Professors, Dept. Eng. Alimentos–UNESP–Rua
Cristovão Colombo, 2265- 15054-000 S.J. Rio Preto, SP, Brasil. (3)
Corresponding author. Fax: +55(17)221–2299. E-mail:
<lopes@eta.ibilce.unesp.br> Cereal Chem. 81(3):369-376. Accepted January
14, 2004. Copyright 2004 American Association of Cereal Chemists, Inc.
Physicochemical properties of maize starch obtained under different steeping
conditions by intermittent milling and dynamic steeping process (IMDS) were
studied. Brazilian dent maize (hybrid XL 606) was milled using a 2×2×3
factorial experimental design with two lactic acid levels (0.0 and 0.55%, v/v),
two SO(2) levels (0.05 and 0.1%, w/v), and three temperatures (52, 60, and
68°C). Properties of starch obtained by conventional wet-milling process (36 hr
at 52°C, 0.55% lactic acid, and 0.2% SO(2)) were used for comparison. Starch
protein content and solubility increased with presence of lactic acid, while
swelling power decreased. Higher SO(2) concentration (0.1%) had the same effect
as lactic acid on some properties. Steeping temperatures of 60 and 68°C
increased solubility and most of the thermal properties but reduced swelling
power, suggesting stronger starch annealing during IMDS at these temperatures.
Some thermal changes on starch granules were visualized by scanning electron
microscopy (SEM) at 60 and 68°C. Amylose content as well as pasting properties
were affected by steeping factors and interactions. Starches from IMDS and
conventional wet-milling processes were similar in most properties, indicating
that IMDS provides starch with quality similar to that from conventional
milling.
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